Apr 24 2024

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   Manufactured from ESR 316 L SS material stock provided by Matt
   Machined to 16 finish (16 micro-inches RMA)
   Polished in the lathe with 400, then 800 grit sandpaper, then diamond paste (5 micron) and finally buffered with cloth, lathe running at 800 rpms. This was very effective at removing machining marks
   Barrel polished: 2 hours coarse (green) cones, followed by 2 hours in fine (red) cones, and finished with 2 hours in corncob. This polishing process rendered the best finish I have seen bringing up the “orange peel” surface look characteristic of diamond paste polishing by hand.
   UHV clean in the SRF chem room
   Vacuum firing to 950 C for 4 hours, still per Tom Elliiot’s protocol.

The vacuum firing turns the electrodes’ surface from shiny to hazy. The same happened to the electrode set (ball, triple point junction shield, back and front end (25 deg Pierce)) used in the R30-3 gun. These electrodes were conditioned to 247 kV and demonstrated field emission free operation at up to 220 kV. So, hazy electrodes are ok for high voltage. The four new electrode pieces show also a haze, but the size of the snowflake-like surface is larger than that seen in the R30-3 gun electrodes. See attached pictures for comparison. Zoom in to see them in detail. The surface finish in the four new pieces looks great in terms of smoothness, in fact, better than the 25 deg Pierce piece used in the R30-3 gun. The only difference is the type of material, I think all of the R30-3 gun electrodes were made from regular 316 L SS.

Joe pointed out that maybe you are observing the diffusion of carbides or other oxides which remain in the ESR (heated under air) to the grains. I doubt it's ~our JLab contamination, rather process materials. Carlos' mentioned main issue found when subjecting the metal to high temperature is reducing the hardness, which I do not see as a problem for high voltage performance.

Vince worked on the 16/30 that did not fit. He opened up the ID successfully, nevertheless it seems that the bolt holes are smaller than they should.

Pictures

  • R30 HVC view of fixture v1 1 feet upstreaam to the left downstreaam to the right.jpg
  • R30-3 gun, 25 deg cone anglec 60 deg junction angle
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  • R30-4 Spare, 16 deg cone angle, 30 deg junction angle IMG 0738.jpg


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